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Apinan Soottitantawat. Synthesis of 7-hydroxy-4-chloromethyl coumarin in stirred tank reactor. (). King Mongkut's University of Technology North Bangkok. Central Library. : , 2017.
Synthesis of 7-hydroxy-4-chloromethyl coumarin in stirred tank reactor
Name: Parada Jungsura
Organization :
Chulalongkorn University. Faculty of Engineering
Name: Uracha Ruktanonchai
Organization :
National Science and Technology Development Agency. National Nanotechnology Center
Name: Khomson Suttisintong
Organization :
National Science and Technology Development Agency. National Nanotechnology Center
Name: Apinan Soottitantawat
Organization :
Chulalongkorn University. Faculty of Engineering
Email :
Apinan.s@chula.ac.th
keyword:
Stirred tank reactor
Abstract:
Coumarins are important groups of naturally occurring compounds. However, they
have been synthetically produced for many years for commercial use. Coumarin and its
derivatives have been studied for physiological activity. Applications of coumarin derivatives
could be found in pharmaceutical, fragrance, agrochemical industries, optical brightening
agent, dispersed fluorescent and anticoagulant. Among the various coumarin derivatives, 7-
hydroxy-4-methylcoumarin is the most widely used one in fine chemical industries. It is
applied to photo-cleavage for drug delivery systems and cytostatic activity. It acts as a
starting material in the preparation of insecticide hymecromone. In this study, 7-hydroxy-4-
chloromethyl coumarin was formed by the chemical reaction between resorcinol and ethyl-4-
chloroacetoacetate with sulfuric acid as a solvent catalyst. The effect of reaction parameters
as temperature and reaction time on product yield as well as product purity were investigated.
The resorcinol was first dissolved in sulfuric acid, then the ethyl-4-chloroacetoacetate was
added to the solution. The highest yield of 70-73% was found at -5-0 ℃. The optimal reaction
time was 2-5 hours because substance is not decomposed in this condition.
King Mongkut's University of Technology North Bangkok. Central Library
Address:
BANGKOK
Email:
library@kmutnb.ac.th
Created:
2017
Modified:
2562-08-05
Issued:
2019-08-05
บทความ/Article
application/pdf
BibliograpyCitation :
In Chemical Society of Thailand under the Patronage of Her Royal Hghness Princess Chulabhorn Mahidol and King Mongkut's University of Technology North Bangkok Faculty of Applied Science. Pure and Applied Chemistry International Conference (PACCON 2017) (pp.390-395). Bangkok : Chemical Society of Thailand under the Patronage of Her Royal Hghness Princess Chulabhorn Mahidol
eng
©copyrights King Mongkut's University of Technology North Bangkok
RightsAccess:
ใช้เวลา
0.024877 วินาที
Parada Jungsura
| Title | Contributor | Type |
|---|---|---|
| Synthesis of 7-hydroxy-4-chloromethyl coumarin in stirred tank reactor
มหาวิทยาลัยเทคโนโลยีพระจอมเกล้าพระนครเหนือ Parada Jungsura;Uracha Ruktanonchai;Khomson Suttisintong;Apinan Soottitantawat | บทความ/Article |
Uracha Ruktanonchai
| Title | Contributor | Type |
|---|---|---|
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| Synthesis of 7-hydroxy-4-chloromethyl coumarin in stirred tank reactor
มหาวิทยาลัยเทคโนโลยีพระจอมเกล้าพระนครเหนือ Parada Jungsura;Uracha Ruktanonchai;Khomson Suttisintong;Apinan Soottitantawat | บทความ/Article | |
| Synthesis of 7-hydroxy-4-chloromethyl coumarin grafted with Indole-3- butyric acid
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Apinan Soottitantawat
| Title | Contributor | Type |
|---|---|---|
| Synthesis of 7-hydroxy-4-chloromethyl coumarin in stirred tank reactor
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